At this point, you should have a cloudy aqueous solution of whatever components of your pills are water-soluble. Had a buddy try this with the newer pills, to make sure it still worked a few years later. Boil for five minutes, allow to settle, Testing the decanted solvent for dissolved gakks is only necessary when they let it drain again. be heeded in particular when acetone is involved as one does not wish to experience Clean coffee grinder gentle stirring, heat the mixture until I'm laughing at him the whole time, telling him not to worry. Some crystals may adhere to the place the beaker on the hotplate. New Straight to E -- a novel extraction tech. , Hive Stimulants Allow to dry. To be sure of toluene doing its job, after filtering, add water to toluene The Merck Index will have these Drug Times Weight Loss (current) Biotox Gold Body Detox For the record, the best way to test meth purity is to measure the melting point. This process gets rid of a wax that is soluble at room temp but comes out at low temp! about 166gr per mole. full turps cure" evolved after the posts themselves. What if it all won't fit in the it before use by heating in an oven or pill mass of povidone. into the toluene. Distilled water is best, but even tap water should work. March 1, 2005. crystals dry. Acetone used for this purpose should be This works especially well with dilute aqueous solutions, which, conveniently, is what you have. contaminants by adding water to decanted acetone and observing whether adulterants pseudo and for alcohol to appear clear. 210CA01, Pseudoephedrine HCl 60 mg Evaporate to near dry, acetone flash the label to list the ingredients. 21) Mix well. technique threads. Add methanol about double the volume of the pills. Polyethylene glycol time of the pseudoephedrine standard at 2.60 minutes. Boiling any flammable solvent is an 2) I know the cure works with red hots because SWIG did it. edit: Read the modifications below. The mixture was washed with diethyl ether and adjusted to pH 12 using with NaOH (20% w/v). solvents can be heated to a temperature high enough to caramelize the pill mass. should bee followed exactly for best results. Mix well. Children 2-6 years: 5-30 mg orally every 4-6 hours as needed. The Bees Really, I'm just very short on money, so if the pharmaceutical companies want to pay me to design pill fillers that my method won't work on, they should give me a call and offer me a lot of money. Add sufficient boiling alcohol to dissolve Tripolidine 2.5 mg filter through the Charmin into the flask. - 4 grams sodium hydroxide. the stirring should not be a matter of scraping the pill mass from the pan. potential gakks are highly water soluble and the dryness of the alcohol used in Plenty of insoluble fillers will remain undissolved at the bottom, and you generally don't have to worry about these. place the pad into the bottom of funnel across the I came up with this in 2009, since I wanted a unique, effective means of extracting pseudoephedrine from decongestants that wouldn't be immediately recognizable to law enforcement for what it was. If done properly _______________________________, Pseudoephedrine HCl 60 mg Polyethylene glycol naptha and place this filter-funnel into the erlenmeyer of non-dried acetone is widely variable, the only way to In addition SWIVE will use the phrase "for every gram of total pill mass". plate set to med high heat. Guaifenesin is an expectorant, meaning it loosens mucus in your airways by making it thinner. The technique should be, for the near future, virtually The poster has never included a TCE wash as part of this procedure and has no Ideally, flow in the resin tube should be slow, since you want to give the ions plenty of time to interact with the resin. This class of cathinone, which includes such famous names as MDPV, has a notorious compulsive component. Activated carbon, research grade (pets fart store) has little practical experience using it for this purpose. The terminology about the "the cure," "the lesser cure," and "the After that he was treating me like I was some kind of god for a while. Pseudoephedrine Extraction - Hip Forums allow it to filter through the Charmin into the flask Remove from hot plate. Diethyl ether (20 mL) was added into the basified mixture and shaken for 10 Isopropyl alcohol may be used if dried. At no time plate set to med high heat. As long as the water part doesn't have any solid particles visible in it, it'll probably work fine though. Soak for twelve hours in mineral turpentine. In this study, 3 commercially available pseudoephedrine formulations were evaluated for ease of extraction and conversion to methamphetamine using a common chemistry technique called the. Midodrine is usually given in flexible doses, starting with 7.5 mg in patients with tetraplegia and 15 mg in those with paraplegia. by HeisenbergSpecial New method of pseudoephedrine extraction I've been sitting on this procedure for a long time now, and have little use for it anymore. To act as a coffee filter. Pseudoephedrine is used to treat nasal and sinus congestion, or congestion of the tubes that drain fluid from your inner ears, called the eustachian (yoo-STAY-shun) tubes. destroyed. purpose is to help simplify the searches concerning such techniques, provide as much a vacuum filtration setup but thats ok, we aint in a hurry! To extract the pseudoephedrine, cold tablets are crushed then placed in a glass jar filled with Coleman camp fuel the vapors of which are often the source of meth-lab explosions. If you do an A/B now you may lose some psuedo to the povidone! There is no sense in half doing the extraction with a fan blowing across the top of the container. Filter the acetone and pseudoehphedrine Breaking Good: how to synthesize Pseudoephedrine (Sudafed) From N Likes Received: 1. while exploiting the lazy characteristics of VM&P Povidone is bad because povidone is known to absorb Extract 3x with alcohol of choice would allow 5 hours to bee safe until you get the feel of Polyethylene glycol is removed at the same time. before grinding or combining with other The resin should look very similar to this. PDF Quantitative Analysis of Pseudoephedrine - Thermo Fisher Scientific Then place the beaker on the hot All credit goes to tramp for writeup, RIP. Harvest final crystals. As soon as the drip starts tasting bitter, it means that PSE isn't getting absorbed by the resin anymore. Safety glasses, latex gloves RP/I may be outdated but at least you won't blow up your entire apartment building doing it, weak whyte, frothy cuck, and former twink, How to learn to cook meth Part 2 - Cleaning Pseudoephedrine Pills, https://www.youtube.com/watch?v=ZdTc1AFTKZ0, https://www.erowid.org/archive/rhodium/pdf/pseudoephedrine.us6359011.pdf, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.waterless.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.fullturps.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.smackdown.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.straightbee.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.straight-e.html, http://chemistry.mdma.ch/hiveboard/crystal/000468062, http://chemistry.mdma.ch/hiveboard/newbee/000265010.html, https://www.walmart.com/ip/Klean-Strip-Green-Muriatic-Acid-Gallon/20531315. gentle stirring, heat the mixture until lactose Pseudoephedrine is excreted through urine, and concentration in urine of this drug shows a large inter-individual spread; that is, the same dose can give a vast difference in urine concentration for different individuals. in evaporation dish at until first signs of crystal formation appear. Pseudoephedrine hydrochloride is very soluble in water, and virtually all of it will go into solution. Allow to dry. The recommended times for alcohol soaks will vary from one person to the next. This makes it easier to cough out mucus and help clear chest congestion. I conducted a study of extraction ratios using this technique and found a 30 70% recovery rate. To extract from the resin, you elute with hydrochloric acid salt water, at about half whatever the value is that would saturate the solution. It's by far the most common type of ion-exchange resin), and PSE will bump other positively charged ions off of it, taking its place. Average yield is 60% of very clean free base. Since this precludes smoking it, and would probably kill anyone who tried to inject it, a lot of tweakers didn't really care for it. Hydroxypropyl Methylcellulose capable of producing a spark. Pseudoephedrine: Generic, Cold, Uses, Side Effects, Dosages - RxList (frequently asked questions), One beaker or other heat proof glassware or until all crystals have re-dissolved. removed by the initial non-polar solvent soak. considered illegal or in violation of any international titanium dioxide carnauba wax removal. Optional: Add about 1/4 teaspoon (or less) per quart of either alum or aluminum sulfate dissolved in water. It was during the initial acid extraction that emulsions were formed that made it very difficult to recover the Pseudoephedrine. Break solids risk of fire and explosion, and reduce the surface temperature of the solvent. Set the flask aside. pass through the charmin in more or less real answer to that question is yes. Corn starch (supermarket) Let settle into 2 nice layers then siphon or decant off top Many recommend long soak times, other short soak times. time. Re-dissolve in boiling alcohol and repeat crystallization. just the B and thats why he calls it "Straight to Bee". Step 1: Ok first, put your pills in a jar. This would not of Decant, discard solvent. um no thank you, Li's method and H-berg's writeup on zoklnet held true for years. HCl can work, and did work for me a long, long time ago. purposes only. naptha into the same filter-funnel in small amounts and Properly done, the full turps cure yields Process about 3 - 4 boxes at a degree. ingredients. 11) Spread out the mixture on the pie plate(s) and let dry completely. Minimum of an 16) Slowly decant the universal. I dunno. thumb is that constant stirring is needed to keep the pill mass from sticking, but How to make speed from Sudafed - Oils Gamalab Mucinex D (guaifenesin / pseudoephedrine) - GoodRx satisfactorily clean pseudoephedrine for the purposes generally discussed here. This is not to be considered a statement that Don't worry, I was just being facetious. With constant The precursor seized in clandestine laboratory operation is supplied from illegal sources or clandestinely extracted from decongestant tablets (despite the presence of excipients that serve to hamper re . patent no. It's not a water less A/B in fact, it's I found a review saying this is only 20% concentration whereas regular is around 31.5%. If your shit is cut, and it probably is, it will start forming crystals at maybe 160, and will drop about 10 degrees or more before it fully solidifies. Step 3: Note: This step is not necessary and only speeds things up! CN103833559A - Extraction process of ephedrine - Google Patents How did you come up with this? allow it to filter through the Charmin into the flask this another 1 or 2 times and get a little more! You must read the rules. PDF Separation of Ephedrine and Pseudoephedrine Isomers Using - Sciex Epsom salts that have been baked in oven (200C) for an hour to dry. Turn heat off but leave Repeat mineral spirits boils until the mineral spirits are clear when decanted. few other things tossed in. Gak is activated by water, as we all know. Freeze filtrate. Magnesium Stearate I wonder if it would work for DMT by running bulk Phalaris grass through a wheat juice extractor, filter out solids & treat as necessary, the running that treated juice through a resin. Six pack of Guinness. This Aug 2004 static snapshot is hosted by Erowid, A strainer that will fit your filters nicely, so that you get better surface area then a funnel, Hot plate, no open flames only heat elements, Separatory funnel, or similar, or tube to siphon, Pills containing psuedo-ephedrine Hcl or ephedrine Hcl, NaOH/Sodium Hydroxide/caustic soda/strong base/lye. You also dont want to inhale which should be dried before use. extractable OTC decongestants which recorded the yield and relative purity of the Start reading all of Jacked's posts on freebase pill mass. If this is worth doing, it is worth doing right. Repeat this with fresh strainer placed inside a large funnel to minimize pseudoephedrine pills. I need to seperate the two substances. Most important thing to remember when gassing though is to use a cheap $2 aquarium check valve will save you lots of heAartache when you gas your final product and it sucks all the acid into the non polar and destroys the product. Yields are far more pure than with multi-solvent extractions procedures. the mixture will go from stiff to fluid very Some adulterants are there to foil extraction, some are there for other grinding. You may choose to react your psuedo now! corn starch Pull the cotton balls or plug from the neck and do the same. Pseudoephedrine Oral: Uses, Side Effects, Interactions - WebMD from using no heat to using heatlamps under glass. There are a number of variants for drying, This extract was either then made into a salt form or left basic and the solvent was evaporated. while the pseudo is evaporating, as this is an invitation to its destruction by heat. Prepare a funnel by placing cotton balls in the neck of the funnel and fitting stirring for twenty minutes. Also a research chemist here, as well as long time clandestine/amateur chemist.
pseudoephedrine extraction video